Patent application number | Description | Published |
20090166916 | Processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization - The present invention provides a processing method of the natural cellulose fiber with feature for enhancing the capability of antifungi, antibacteria and deodorization. The procedure is that firstly modify and reduce the properties of the natural chitosan of high polymer material to nanometer scale; secondly dunk the chitosan into the syrup-like mixture of wood pulp and NMMO solvent to yield quasi-dope; thirdly dehydrate the quasi-dope of paste mixture to form the mud-like dope; fourthly spin the dope by dryjet wet spinning method; fifthly regenerate the filament in coagulation bath, water rinse and dry; finally water rinse, dry, apply the lubricant to finish. The water soluble chitosan, which has been treated by property modification and reduced to nanometer scale, can effectively and completely solve in the cellulose of low DP to offer wider extent of selection in the DP and better flexibility of adding percentage in content of modified chitosan. | 07-02-2009 |
20110154627 | Meltblown wetlaid method for producing non-woven fabrics from natural cellulose - The present invention provides a meltblown wetlaid method for producing non-woven fabrics from natural cellulose using pulp as raw material and N-methylmorpholine N-oxide (NMMO) as solvent for dissolving into dope. The dope is then extruded out of a spinneret to form filament bundle by meltblown method. Subsequently, by means of ejecting mist aerosol of water, the filament bundle is coagulated with regeneration. Via post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like have been orderly applied, then final product of nonwoven fabrics with continuous filament are produced from natural cellulose. | 06-30-2011 |
20110156299 | MELTBLOWN WETLAID METHOD FOR PRODUCING NON-WOVEN FABRICS WITH ANTI-MILDEW, ANTI-BACTERIA AND DEODORIZING CAPABILITIES FROM NATURAL CELLULOSE - The present invention provides a meltblown wetlaid method for producing non-woven fabrics with anti-mildew, anti-bacteria and deodorizing capabilities from natural cellulose. The method comprises selecting wood pulp as raw material and using N-methylmorpholine N-oxide (NMMO) as dissolving solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as stabilizer to form mixed cellulose mucilage as well as using modified and nano-miniaturized natural chitosan as additive for blending and dissolution to form cellulose dope. By meltblown method, the dope is extruded out of spinnerets to form filament bundle, then by ejecting mist aerosol of water, the filament bundle is coagulated with regeneration. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like having been orderly applied, then final product for nonwoven fabric of continuous filament with anti-mildew, anti-bacteria and deodorizing capabilities is produced. | 06-30-2011 |
20110156303 | SPUNBOND WETLAID METHOD FOR PRODUCING NON-WOVEN FABRICS FROM NATURAL CELLULOSE - The present invention provides a “spunbond wetlaid method for producing non-woven fabrics from natural cellulose” using pulp as raw material and N-methylmorpholine N-oxide (NMMO) as solvent for dissolving into dope. Then, the dope is extruded out of a spinneret to form filament bundle by spunbond method. The dope is extruded out of a spinneret bank of grouped spinnerets to form filament bundle for further stretching process under quench condition. The filament bundle is coagulated with regeneration in a coagulating solution. The coagulated filament bundle is rapidly stretched under high pressure by an air draw-off machine. The stretched filament bundle is collected and stacked on a collecting net as web nonwoven. After post treatments of water rinsing, hydro-entangled needle punching, drying, winding-up and the like have been orderly applied then final product of nonwoven fabrics with continuous filament are produced from natural cellulose. | 06-30-2011 |
20130062566 | Method of Recovering and Concentrating an Aqueous N-methylmorpholine-N-Oxide (NMMO) Solution - This disclosure relates to a method of recovering and concentrating an aqueous N-methylmorpholine-N-oxide (NMMO) solution. | 03-14-2013 |
20130228949 | FABRICATION OF NATURAL CELLULOSE FIBER WITH FLAME-RETARDING CAPABILITY - A fabrication of natural cellulose fiber with flame-retarding capability comprises following steps. Blend pulp and solvent of N-methylmorpholine N-oxide (NMMO) to form slurry. Evaporate extra water content from slurry by a Thin Film Evaporator (TFE) to form dope. By Dry-Jet Wet Spinning, spin and extrude dope for coagulating and regenerating. Water-rinse and dry to form natural cellulose fiber. Soaking roll natural cellulose fiber by flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl). Orderly dry, bake, neutralize, soaping clean, water rinse, baking dry, soaking rolled, alkaline clean, water rinse, dry and oil the natural cellulose fiber to produce natural cellulose fiber of flame retarding capacity. Because of cross-linking reaction for the flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl) with natural cellulose fiber, the flame-retarding capability thereof meet requirements of testing standards in American ASTM D6413-1999 and ASTM D2863-1995. Moreover, the wastes thereof meet the requirements of environment protections without harm. | 09-05-2013 |
20130234354 | MELTBLOWN PROCESS FOR PRODUCING NON-WOVEN FABRICS WITH FLAME-RETARDING CAPABILITY FROM NATURAL CELLULOSE - A Meltblown process for producing non-woven fabrics with flame-retarding capability from natural cellulose comprises following steps. Blend pulp and solvent of N-methylmorpholine N-oxide (NMMO) to form slurry. Evaporate water content from slurry by a Thin Film Evaporator to form dope. Extrude the dope off spinneret bank to form filament bundle via meltblown process. Coagulating regenerate, water rinse, hydro-entangled needle-punch and dry the filament bundle to form normal natural cellulose nonwoven. Soaking roll formed nonwoven by flame retardant of N-(hydroxymethyl)-3-(methoxy phosphorus acyl). Orderly dry, bake, neutralize, soaping clean, water rinse, baking dry, soaking roll, alkaline clean, water rinse, dry and coil the nonwoven to produce modified natural cellulose nonwoven of flame retarding capacity. Because of cross-linking reaction between foregoing flame retardant and natural cellulose nonwoven, the flame-retarding capability thereof meet requirements of testing standards in American ASTM D6413-1999 and ASTM D2863-1995. Moreover, the wastes thereof meet environmental protection requirements. | 09-12-2013 |
20140008577 | Method of Recovering Aqueous N-Methylmorpholine-N-Oxide Solution Used in Production of Lyocell Fiber - A method of recovering aqueous N-Methylmorpholine-N-Oxide solution used in production of Lyocell fiber comprises following steps. Bleach means for decoloring coloration in aqueous NMMO solution via alternate blow-mixing adsorption mode and static suspending adsorption mode reiteration. Filtration means for purifying the activated carbon powder and impurities by two filtering stages of first coarse filtering stage and second fine filtering stage. Concentration means for intensifying aqueous NMMO solution to obtain a condensed aqueous solution without NMMO solvent and a concentrated aqueous solution with NMMO solvent respectively by a sequential multi-stage evaporating system. Refinement means for purifying aqueous NMMO solution with promoting purity of concentrated aqueous solution to obtain required recovered aqueous solution by adding suitable agents in the redox reactions involved. Owing to streamlining and simplicity, the method not only has better competitiveness from promoted recovery cost, efficiency and quality but also meets regulations of environmental protection. | 01-09-2014 |
20140165463 | Producing method for the artificial peat moss from natural cellulose fiber - The present invention provides a producing method for the artificial peat moss from natural cellulose fiber. The producing method comprises following steps in successive order manner. Firstly, blend natural pulp with N-methylmorpholine N-oxide (NMMO) as dissolving solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as stabilizer in proper mixing ratio to yield a preliminary quasi-dope. Secondly, stir and dehydrate the preliminary quasi-dope to form dope. Thirdly, spin the dope by dry jet wet spinning method to yield filament bundle of cellulose. Fourthly, orderly perform coagulating with regenerating, water rinsing, twisting with plying and cutting processes on the filament bundle of cellulose to yield a preliminary artificial peat moss of natural cellulose fiber. Finally, per drying process of post-treatment on the preliminary artificial peat moss of natural cellulose fiber to obtain final artificial peat moss of natural cellulose fiber of the present invention. | 06-19-2014 |
20140291882 | Processing method of natural cellulose fiber intrinsically with enhanced antiseptic, deodorant and negative-ion features from bamboo - The present invention provides a processing method of natural cellulose fiber intrinsically with enhanced antiseptic, deodorant and negative-ion features from bamboo. The process uses mixture of wasted coffee residue and bamboo pulp as raw material. The process uses N-methylmorpholine N-oxide (NMMO) as primary solvent and 1, 3-phenylene-bis 2-oxazoline (BOX) as additive stabilizer. A cellulose solution is firstly formed by the wasted coffee residue, bamboo pulp, NMMO and BOX aforesaid. Secondly, via grinding, blending, dissolving and thermal dehydrating, the cellulose solution is converted into spinning dope. Thirdly, spin the dope obtained previously by dry-jet wet spinning method and coagulate and regenerate in a coagulation bath to form into threads. Finally, rinse, desiccate and lubricate the regenerated threads obtained previously as well as wind it up to produce reeled natural bamboo cellulose fiber with enhanced antiseptic, deodorant and negative-ion features. | 10-02-2014 |
20140291883 | Processing method of non-woven intrinsically with enhanced deodorant feature from bamboo - The present invention provides a processing method of non-woven intrinsically with enhanced deodorant feature from bamboo. The process uses mixture of wasted coffee residue and bamboo pulp as raw material. The process uses N-methylmorpholine N-oxide (NMMO) as primary solvent and 1,3-phenylene-bis 2-oxazoline (BOX) as additive stabilizer. A cellulose solution is firstly formed by the wasted coffee residue, bamboo pulp, NMMO and BOX aforesaid. Secondly, via grinding, blending, dissolving and thermal dehydrating, the cellulose solution is converted into spinning dope. Thirdly, via meltblown method, the dope is extruded out of spinnerets in a die assembly by a metering gear pump to form thread bundle. Finally, the thread bundle is orderly treated by coagulation with regeneration via ejecting mist aerosol of water, rinsing, bleaching, re-rinsing, drying, winding-up and the like to create continuous filaments, then final product for nonwoven with deodorant feature is produced by the filaments from bamboo cellulose. | 10-02-2014 |