Patent application number | Description | Published |
20080260566 | METHOD FOR PRODUCING A METALLIC ARTICLE HAVING A GRADED COMPOSITION, WITHOUT MELTING - A method for preparing a metallic article made of metallic constituent elements includes furnishing a chemically reduced initial metallic material formed from chemically reducing a mixture of nonmetallic precursor compounds of the metallic constituent elements, without melting the initial metallic material, and consolidating the initial metallic material to produce a consolidated metallic article, without melting the initial metallic material and without melting the consolidated metallic article. A net macroscopic composition of the consolidated metallic article varies spatially according to a pre-selected pattern | 10-23-2008 |
20080292488 | METHOD FOR PREPARING A METALLIC ARTICLE HAVING AN OTHER ADDITIVE CONSTITUENT, WITHOUT ANY MELTING - A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article. | 11-27-2008 |
20090032152 | METHOD FOR PRODUCING A BETA-PROCESSED ALPHA-BETA TITANIUM-ALLOY ARTICLE - A titanium-alloy article is produced by providing a workpiece of an alpha-beta titanium alloy having a beta-transus temperature, and thereafter mechanically working the workpiece at a mechanical-working temperature above the beta-transus temperature. The mechanically worked workpiece is solution heat treated at a solution-heat-treatment temperature of from about 175° F. below the beta-transus temperature to about 25° F. below the beta-transus temperature, quenched, overage heat treated at an overage-heat-treatment temperature of from about 400° F. below the beta-transus temperature to about 275° F. below the beta-transus temperature, and cooled from the overage-heat-treatment temperature. | 02-05-2009 |
20100258260 | PRODUCING METALLIC ARTICLES BY REDUCTION OF NONMETALLIC PRECURSOR COMPOUNDS AND MELTING - A metallic article is produced by furnishing one or more nonmetallic precursor compound comprising the metallic constituent element(s), and chemically reducing the nonmetallic precursor compound(s) to produce an initial metallic particle, preferably having a size of no greater than about 0.070 inch, without melting the initial metallic particle. The initial metallic particle is thereafter melted and solidified to produce the metallic article. By this approach, the incidence of chemical defects in the metal article is minimized. The melted-and-solidified metal may be used in the as-cast form, or it may be converted to billet and further worked to the final form. | 10-14-2010 |
20100288075 | METHOD FOR PRODUCING A TITANIUM-BASE ALLOY HAVING AN OXIDE DISPERSION THEREIN - A metallic article is prepared by first furnishing at least one nonmetallic precursor compound, wherein all of the nonmetallic precursor compounds collectively containing the constituent elements of the metallic article in their respective constituent-element proportions. The constituent elements together form a titanium-base alloy having a stable-oxide-forming additive element therein, such as magnesium, calcium, scandium, yttrium, lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, and lutetium, and mixtures thereof. The stable-oxide-forming additive element forms a stable oxide in a titanium-based alloy. At least one additive element is present at a level greater than its room-temperature solid solubility limit in the titanium-base alloy. The precursor compounds are chemically reduced to produce an alloy material, without melting the alloy material. The alloy material may be consolidated. The alloy material, or consolidated metallic article, is thereafter desirably exposed to an oxygen-containing environment at a temperature greater than room temperature. | 11-18-2010 |
20120263619 | METHOD FOR PREPARING A METALLIC ARTICLE HAVING AN OTHER ADDITIVE CONSTITUENT, WITHOUT ANY MELTING - A method for preparing an article of a base metal alloyed with an alloying element includes the steps of preparing a compound mixture by the steps of providing a chemically reducible nonmetallic base-metal precursor compound of a base metal, providing a chemically reducible nonmetallic alloying-element precursor compound of an alloying element, and thereafter mixing the base-metal precursor compound and the alloying-element precursor compound to form a compound mixture. The compound mixture is thereafter reduced to a metallic alloy, without melting the metallic alloy. The step of preparing or the step of chemically reducing includes the step of adding an other additive constituent. The metallic alloy is thereafter consolidated to produce a consolidated metallic article, without melting the metallic alloy and without melting the consolidated metallic article. | 10-18-2012 |
20130302645 | ARTICLE HAVING A DISPERSION OF ULTRAFINE TITANIUM BORIDE PARTICLES IN A TITANIUM-BASE MATRIX - An article includes a microscale composite material having a matrix with titanium boride particles configured to form an insert in a metallic mass being comprised of material other than a consolidated titanium-based metallic composition having titanium particles. | 11-14-2013 |
Patent application number | Description | Published |
20110257008 | METHOD FOR MAKING HIGHLY POROUS, STABLE METAL OXIDES WITH A CONTROLLED PORE STRUCTURE - Methods for making high-surface area, high-porosity, stable metal oxides, such as, but not limited to materials used as adsorbents and catalyst supports include (i) forming a solvent deficient precursor mixture from a metal salt and a base and reacting the metal ions and base ions in the solvent deficient precursor mixture to form an intermediate hydroxide product (e.g., metal hydroxide or metal oxide hydroxide), (ii) causing the intermediate hydroxide to form nanoparticles (e.g., by heating), and (iii) calcining the intermediate nanoparticles to sinter the nanoparticles together and yield a highly porous, stable metal oxide aggregate having a pore structure. | 10-20-2011 |
20130267411 | SINGLE REACTION SYNTHESIS OF TEXTURIZED CATALYSTS - Methods are described for making a texturized catalyst. The textural promoter may be a high-surface area, high-porosity, stable metal oxide support. The catalyst is manufactured by reacting catalyst precursor materials and support materials in a single, solvent deficient reaction to form a catalyst. The catalyst may be particles or a coating or partial coating of a support surface. | 10-10-2013 |
20130274093 | IRON AND COBALT BASED FISCHER-TROPSCH PRE-CATALYSTS AND CATALYSTS - A method of making iron and cobalt pre-catalysts and catalysts in activated, finished form suitable for use in Fischer-Tropsch synthesis. The pre-catalysts are prepared by mixing an iron or cobalt salt, a base, and a metal oxide textural promoter or support. The reaction is carried out in a solvent deficient environment. The resulting product is then calcined at temperatures of about 300-500° C. to produce a metal oxide. The catalysts are prepared by reducing the metal oxide in the presence of hydrogen at temperatures of about 300-500° C. and carbiding the reduced metal in the case of iron. | 10-17-2013 |
20140256543 | METHOD OF MAKING HIGHLY POROUS, STABLE ALUMINUM OXIDES DOPED WITH SILICON - The present invention relates to a method for making high surface area and large pore volume thermally stable silica-doped alumina (aluminum oxide) catalyst support and ceramic materials. The ability of the silica-alumina to withstand high temperatures in presence or absence of water and prevent sintering allows it to maintain good activity over a long period of time in catalytic reactions. The method of preparing such materials includes adding organic silicon reagents to an organic aluminum salt such as an alkoxide in a controlled quantity as a doping agent in a solid state, solvent deficient reaction followed by calcination. Alternatively, the organic silicon compound may be added after calcination of the alumina, followed by another calcination step. This method is inexpensive and simple. The alumina catalyst support material prepared by the subject method maintains high pore volumes, pore diameters and surface areas at very high temperatures and in the presence of steam. | 09-11-2014 |